Technical Information
2) Bottle Sampler
Technical Information
1) LPA2
(For Bottle Sampler Technical Information, see below)
Unit Type
ISO 4406 Code
PUMP Piston (slow speed, inline)
Piston (high speed, variable)
Gear
Vane
22/20/16

17/15/13

19/17/15
18/16/14
MOTOR Axial piston
Radial piston
Gear
Vane
18/16/13
19/17/13
20/18/15
19/17/14
VALVE Directional (solenoid)
Pressure control (modulating)
Flow control
Check valve
Cartridge valve
Proportional
Servovalve
20/18/15

19/17/14

19/17/14
20/18/15
20/18/15
18/16/13
16/14/11
ACTUATOR  
20/18/15

Typical Manufacturer's Recommendations for Component Cleanliness (ISO 4406)

It should be noted that the recommendations made in this table should be viewed as starting levels and may have to be modified in light of operational experiences or user requirements.

Hydraulic System Target Cleanliness Levels*

Where a hydraulic system user has been able to check cleanliness levels over a considerable period, the acceptability, or otherwise, of those levels can be verified. Thus if no failures have occurred, the average level measured may well be one which could be made a bench mark. However, such a level may have to be modified if the conditions change, or if specific contaminant-sensitive components are added to the system. The demand for greater reliability may also necessitate an improved cleanliness level.

The level of acceptability depends on three features
•   the contamination sensitivity of the components
•   the operational conditions of the system
•   the required reliability and life expectancy

Contamination
codes
ISO 4406
Correspondent
codes
NAS 1638
Recommended
filtration
degree
Typical applications
4µm(c)
6µm(c)
14µm(c)
 
B x ≥ 200
14
12
9
3
3
High precision and laboratory servo-systems
17
15
11
6
3 - 6
Robotic and servo-systems
18
16
13
7
10 - 12
Very sensitive - high reliability systems
20
18
14
9
12 - 15
Sensitive - reliable systems
21
19
16
10
15 - 25
General equipment of limited reliability
23
21
18
12
25 - 40
Low - pressure equipment not in continuous service

New ISO Standard Test Dust and its effect on ISO Contamination Control Standards

When General Motors gave advance warning to the International Standards Organisation (ISO) that it was intending to stop the production of AC Fine Test Dust (ACFTD), work commenced immediately on finding an improved replacement dust. ACFTD was used extensively within the fluid power and automotive industries for calibrating Automatic Particle Counters (APCs) and for the testing of components. APCs are used for testing oil filters, and also for contaminant sensitivity testing of hydraulic components.

For 25 years, APCs have been the main stay in the measurement of solid particles in hydraulic fluids. The growth in demand for measuring fluid cleanliness in a variety of industrial processes, including fluid power, has resulted in APCs moving from the laboratory environment out into the factory. In fact, they are now a critical part of many production processes. It is therefore essential that the data they provide is both accurate and consistent.

Calibration
ACFTD has been used as an artificial contaminant since the 1960s and its original particles size distribution was determined using an optical microscope. This particle size distribution subsequently formed the basis of ISO 4402, the method for calibrating APCs. Due to the limitations of that method of measurement, the particle size distribution was questioned below about 5 microns. It was also not traceable to any national standard of measurement - a critical requirement for today’s quality management systems.

There was also an absence of formal controls over the distribution of the test dust, and batch-to-batch variability was much greater than is acceptable nowadays.
ISO therefore defined the requirements for the replacement for ACFTD and asked the National Institute of Standards and Technology (NIST) in the USA to produce a standard, traceable reference material. The new dust’s particle size distribution has been accurately determined with the aid of modern scanning electron microscope and image analysis techniques.

New Test Dust Benefits
The new ISO Medium Test Dust (ISOMTD) consists of similar materials to the old ACFTD, but to minimise particle counting errors, it is of a slightly coarser grade because ACFTD included too many particles smaller than 5 microns which gave problems during testing.
ISOMTD is produced to a standard distribution and stringent quality control procedures, thereby ensuring excellent batch-to-batch repeatability. These procedures, combined with a revised ISO APC calibration method give:

•   A traceable and controlled reference test dust with greatly reduced variation in particle size distribution.
    This gives the traceability required by ISO 9000, QS9000 and similar quality management systems.
•   A procedure for determining the performance of APCs so that minimum acceptable levels can be set by
    the user.
•   Improved calibration techniques and procedures.
•   More accurate calibration.
•   Improved levels of particle count reproducibility with different equipment.
•   More accurate and consistent filter test results.

Effect on Industry
The introduction of ISOMTD has necessitated changes to certain ISO standards.
The standards affected include:-

ISO 4402 : 1991 Hydraulic fluid power
                     Calibration of liquid automatic particle counters.

ISO 4406 : 1987 Hydraulic fluid power
                     Code for defining the level of contamination by solid particles.

ISO 4572 : 1981 Hydraulic fluid power                    
                     Filters
                     Multi-pass method for evaluating filtration performance of a filter element.


In order that users are not confused by the changes to these standards, particularly by reference to them in technical literature, ISO is updating 4402 to ISO 11171, and 4572 to ISO 16889.

Two standards which concern our industry are the ISO 4406 coding system and the new ISO 16889 Multi-pass test. As APCs will henceforth count particles more accurately, there will now be a change in the way sizes are labelled.

In the new ISO 4406, new calibration sizes are used to give the same cleanliness codes as the ‘old’ calibration sizes of 5 and 15 microns. In this way, there will be no necessity to change any system cleanliness specifications. It is proposed that the cleanliness codes (for APCs) will be formed from three* particle counts at 4, 6 and 14 microns, with 6 and 14 microns corresponding very closely to the previous 5 and 15 micron measurements. This will ensure consistency in data reporting.

*The option of quoting just two counts of 6 microns and 14 microns for APCs remains.
As the counts derived by microscope counting methods are not affected, the particle sizes used for microscopy will remain unchanged (i.e. at 5 and 15 microns).

To clarify matters still further, ISO standards written around the new test dust will utilise a new identifier, ‘(c)’. Hence micron sizes according to the new ISO 11171 will be expresses as ‘µm(c)’ and Beta ratios according to ISO 16889 will be expressed as ‘Bx(c)’, e.g. ‘B5(c)’.

However, it must be stressed that the only real effect users will experience will be the improved accuracy in particle counts - there will be no change in the performance of filters, nor in the ISO cleanliness levels that they will achieve.

The following charts shows the correlation between the old ACFTD and the new ISOMTD.

The LPA2 is calibrated with ISO Medium Test Dust (to ISO 11171).
The correlation between particle sizes and the ACFTD (old standard) to the ISOMTD (new standard) is as follows :

 

ACFTD
<1
5
15
25
30
50*
75*
100*
ISOMTD
4
16
14
21
25
38  
50  
68  
* To be confirmed by NIST
< select buttons for further information

Calibration between Particle Sizes obtained using ACFTD (ISO 4402:1991) and NIST (ISO 11171) calibration methods *

Particle size obtained using :

ACTFD SIZE
(ISO 4402:1991)
µm
NIST SIZE
(ISO 11171)
µm(c)
1
4.2
2
4.6
3
5.1
4
5.8
5
6.4
6
7.1
7
7.7
8
8.4
9
9.1
10
9.8
11
10.6
12
11.3
13
12.1
14
12.9
15
13.6
16
14.4
17
15.2
18
15.9
19
16.7
20
17.5
21
18.2
22
19.0
23
19.7
24
20.5
25
21.2
26
22.0
27
22.7
28
23.5
29
24.2
30
24.9
31
25.7
32
26.4
33
27.1
34
27.9
35
28.5
36
29.2
37
29.9
38
30.5
39
31.1
40
31.7
This table is only a guideline.

The exact relationship between ACFTD sizes and the NIST sizes may vary from instrument to instrument depending on the characteristics of the particle counter and original ACFTD calibration.

 

* All sections headings indicated with an asterisk are reproduced by kind permission of British Fluid Power Association from BFPA/P5 1999 Issue 3

Other standards

Although ISO 4406 standard is being used extensively within the hydraulics industry other standards are occasionally required and a comparison may be requested. The following table gives a very general comparison but often no direct comparison is possible due to the different classes and sizes involved.

ISO 4406 DEF.STD 05/42 [7] NAS 1638
[5]
ISO 11218
[6]
SAE 749
[8]
13/11/08
-
-
2
-
14/12/09
-
-
3
0
15/13/10
-
-
4
1
16/14/09
-
400F
-
-
16/14/11
-
-
5
2
17/15/09
400
800F
-
-
17/15/10
-
-
-
-
17/15/10
-
-
6
3
18/16/10
800
1,300F
-
-
18/16/11
-
-
-
-
18/16/13
-
2,000F
7
4
19/17/11
1,300
-
-
-
19/17/14
-
-
8
5
20/18/12
2,000
4,400F
-
-
20/18/13
-
-
-
-
20/18/15
-
6,300F
9
6
21/19/13
4,400
-
-
-
21/19/16
-
-
10
-
22/20/13
6,300
-
-
-
22/20/17
-
-
11
-
23/12/14
15,000
-
-
-
23/21/18
-
-
12
-
24/22/15
21,000
-
-
-
25/23/17
100,000
-
-
-
Information from BFPA/P5 paragraph 7.6.2 Sample Bottles and 7.6.3 Sampling Procedures

It is essential that only sample bottles that have been cleaned to ISO 3722 standard are used.

Modern hydraulic systems featuring highly effective filters have fluid cleanliness levels that approach that of the sample bottle themselves.

The use of un-cleaned bottles can greatly increase the particle counts. (Please note sterilisation kills bacteria but does not remove particles). Perhaps of even greater concern is the variability in their levels of cleanliness.

A sudden increase in contamination could be caused by the sample bottle. This apparent increase could instigate unnecessary corrective action.

Table : Cleanliness of sample bottles compared to system levels
Sample
Particle Counts per 100mL
 
>2 µm
>5 µm
> 15 µm
> 25 µm
> 50 µm
Bottles
250mL bottles cleaned to ISO 3772
As received (glass)
As received (plastic)

System Levels
Servo controlled fatigue rig
Plastic injection moulding machines
Agricultural tractors (roll-off) cleanliness
Rail car transmissions


285
5,900
10,150

4,200
7,160
-
12.600

150
3,480
6,615

2,268
2,900
14,200
5,650

26
1,090
2,410

640
784
804
760

7
4 25
1,115

183
192
308
121

0
102
275

24
16
24
6
The sample must be collected in an appropriate manner such that the contribution of extraneous dirt is kept to a minimum. The procedure is defined in ISO 4021 and the salient points are given here:
  • Ensure that any external device (sampler, etc.) is cleaned accordingly.
  • Inspect the sampling valve (or entry point to the reservoir) for settled dirt and flush the externals with filtered solvent (remember individual particles <40µm cannot be seen by the unaided eye).
  • Unscrew the dust cap of the sampling valve (if appropriate) and flush the externals of the valve.
  • Connect the sampler to the valve, and both carefully and slowly open the valve. Adjust the valve so that the flowrate is sufficient for flushing the internal surfaces and its collection. Experience has indicated that 1 to 2 L/min is suitable. The emerging jet should be directed away from the system to avoid dirt that has settled on pipes from being dislodged and falling in to the sampling bottles.
  • Uncap the sample bottle, and take the sample in a continuous manner without making any adjustment to the valve as this can generate contaminant. Do not place the cap on a dirty surface or place it in the upturned position. Fill the sample bottle to about 80% of its volume so that the contents can be redispersed during the analysis stage.
  • When 80% full, withdraw the sample bottle and immediately replace the cap.
  • Turn off the flow, disconnect the sampler and replace the dust cap. Label the sample bottle with details of content and where and when sampled etc.
For modern systems which feature very clean fluids, samples should be taken from the line mounted locations so that the valve can be adequately flushed to ensure that the sample is representative of the main stream. However, it is accepted that not all systems will be fitted with line mounted sampling valves and the reservoir can present an alternative source. This can be achieved by making access to the reservoir, but the following points should be noted:
  • The access hole should be adequately sized to allow the passage of the sampling probe.
  • It should be positioned so that the sample is taken from a centralised region of the reservoir not adjacent to the inlet to the pump or the return pump, and away from any baffles.
  • It should be located in an accessible area which will not accumulate dirt and is free from air currents e.g., electric motor cooling fans.
  • The access hole should be thoroughly cleaned beforehand to avoid dirt being introduced into the reservoir.
  • The access hole should be closed immediately after sampling.

 
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Hydraulic Component Manufacturer’s* Recommendations

Most component manufacturers know the proportionate effect that increased dirt level has on the performance of their components and issue maximum permissible contamination levels. They state that operating components on fluids which are cleaner than those stated will increase life.

However, the diversity of hydraulic systems in terms of pressure, duty cycles, environments, lubrication required, contaminant types, etc, makes it almost impossible to predict the components service life over and above that which can be reasonably expected.

Furthermore, without the benefits of significant research material and the existence of standard contaminant sensitivity tests, manufacturers who publish recommendations that are cleaner than competitors may be viewed as having a more sensitive product.

Hence there may be a possible source of conflicting information when comparing cleanliness levels recommended from different sources.

The table below gives a selection of maximum contamination levels that are typically issued by component manufacturers. These relate to the use of the correct viscosity mineral fluid. An even cleaner level may be needed if the operation is severe, such as high frequency fluctuations in loading, high temperature or high failure risk.

Moisture Sensor